電極的保養(yǎng)和故障排除-深圳市慧聰源環(huán)?？萍加邢薰?/title> <link rel="stylesheet" type="text/css" href="/skins/270528/css/style.css"> <script src="/skins/270528/js/jquery-3.6.0.min.js"></script> <link rel="shortcut icon" href="/skins/270528/favicon.ico">  <script type="text/javascript"> document.addEventListener("touchstart", function () { }, true); </script>  <script language="javascript" type="text/javascript"> var nav= '5'; </script>  <script type="application/ld+json"> { "@context": "https://ziyuan.baidu.com/contexts/cambrian.jsonld", "@id": "http:///szhcy-Article-1917793/", "title": "電極的保養(yǎng)和故障排除", "pubDate": "2019-07-31T17:48:35", "upDate": "2019-07-31T17:48:35" }</script> <script language="javaScript" src="/js/JSChat.js"></script><script language="javaScript">function ChatBoxClickGXH() { DoChatBoxClickGXH('https://chat.chem17.com',262687) }</script><script> (function(){ var bp = document.createElement('script'); var curProtocol = window.location.protocol.split(':')[0]; if (curProtocol 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id="tq6ztn8r" class="ly_NyNewsdetail"> <h1 class="NyNewsdetail_title">電極的保養(yǎng)和故障排除</h1> <div id="tq6ztn8r" class="NyNewsdetail_tips">更新時(shí)間：2019-07-31 點(diǎn)擊次數(shù)：2510</div> <div id="tq6ztn8r" class="NyNewsdetail_con"> <p> 1<span style="font-family:宋體">、</span><strong>pH</strong><strong><span style="font-family:宋體">電極</span></strong><span style="font-family:宋體">的陶瓷隔膜。工業(yè)</span>pH<span style="font-family:宋體">值測(cè)量系統(tǒng)的故障絕大多數(shù)由于</span>pH<span style="font-family:宋體">電極引起，其中又以陶瓷隔膜部分問(wèn)題多，陶瓷隔膜有許多微米級(jí)的孔，必須保持隔膜微孔的暢通，以確保電極的外參比液滲入被測(cè)量溶液中，建立穩(wěn)定的參考電位。陶瓷隔膜目視一般為白色，當(dāng)顏色變黃或褐色甚至黑色時(shí)，陶瓷隔膜孔存在不同程度的堵塞，在校驗(yàn)的時(shí)候表現(xiàn)為對(duì)標(biāo)準(zhǔn)液的響應(yīng)時(shí)間明顯增長(zhǎng)，長(zhǎng)時(shí)問(wèn)難以達(dá)到穩(wěn)定的</span>pH<span style="font-family:宋體">值讀數(shù)，甚至*不能識(shí)別標(biāo)準(zhǔn)液。這時(shí)就需要進(jìn)行電極隔膜的浸泡，以消除這此沉淀，打通陶瓷隔膜的微孔，重新恢復(fù)電極的性能。</span></p><p> 2<span style="font-family:宋體">、</span><strong>pH</strong><strong><span style="font-family:宋體">電極</span></strong><span style="font-family:宋體">的敏感膜。電極的敏感膜會(huì)逐漸老化，使</span>H<sup>+</sup><span style="font-family:宋體">在被測(cè)量溶液及敏感膜之間的擴(kuò)散更加困難，從而導(dǎo)致響應(yīng)時(shí)問(wèn)增長(zhǎng)，所測(cè)量的</span>pH<span style="font-family:宋體">值比實(shí)際值偏高。這時(shí)需要使用含</span>HF<span style="font-family:宋體">的電極敏感膜再生液進(jìn)行處理，由于再生液會(huì)溶蝕敏感膜，并且溶蝕過(guò)程是不可逆轉(zhuǎn)的，所以該處理過(guò)程必須特別小心，一日處理過(guò)度，電極就可能報(bào)廢了。此處理不建議用戶自己做，請(qǐng)把電極交給制造商的專業(yè)技術(shù)人員進(jìn)行處理，專業(yè)技術(shù)人員處理好后出具</span><strong>pH</strong><strong><span style="font-family:宋體">電極</span></strong><span style="font-family:宋體">的處理報(bào)告和使用建議，用戶按處理過(guò)后的技術(shù)報(bào)告重新選擇使用，再生處理后的電極性能不如新的電極，可能需要降低使用的場(chǎng)合，不建議對(duì)電極進(jìn)行多次再生。不要用手直接觸摸電極的連接頭部分和玻璃敏感膜部分。以免污染電極。</span></p><p><span style="font-family:宋體"> 正常情況下，</span><strong>pH</strong><strong><span style="font-family:宋體">電極</span></strong><span style="font-family:宋體">的壽命一般取決于兩個(gè)方面：敏感膜的老化和外參比介質(zhì)的消耗。前面提到，敏感膜的壽命隨介質(zhì)和溫度不同差別較大，在實(shí)驗(yàn)室環(huán)境電極敏感膜的壽命可能達(dá)到三年或者更長(zhǎng)。</span></p><p><span style="font-family:宋體"> 關(guān)于外參比介質(zhì)的消耗，對(duì)液體電極而言，外參比介質(zhì)的消耗可重新添加，因此其壽命</span> <span style="font-family:宋體">較長(zhǎng)。液體電極必須使用原廠提供的外參比液。如果液體電極在使用過(guò)程中異常失壓。導(dǎo)致</span> <span style="font-family:宋體">被測(cè)量介質(zhì)通過(guò)微孔陶瓷隔膜反向滲透至電極外參比液中，可能會(huì)導(dǎo)致外參比液成分改變，</span> <span style="font-family:宋體">參比電極不能正常建立參考電位，從而影響</span>pH<span style="font-family:宋體">值的測(cè)量，這時(shí)需要把電極交給制造商，清空舊外參比液并重新添加新參比液。</span></p><p><span style="font-family:宋體"> 凝膠電極的外參比介質(zhì)不可添加，在未使用前不要開(kāi)啟陶瓷隔膜的密封膠，開(kāi)啟后就要</span> <span style="font-family:宋體">盡快使用，不要在密封膠開(kāi)啟短暫使用后再長(zhǎng)期儲(chǔ)存。由于在電極中對(duì)外參比膠體預(yù)加壓，</span> <span style="font-family:宋體">隔膜的密封膠一開(kāi)啟外參比介質(zhì)就開(kāi)始往外擴(kuò)散消耗，不管該電極是否處于測(cè)量狀態(tài)或儲(chǔ)存</span> <span style="font-family:宋體">狀態(tài)，正常情況下凝膠電極的外參比介質(zhì)可使用一年或以上。固體電極中固化的參比介質(zhì)消</span> <span style="font-family:宋體">耗速度和被測(cè)量介質(zhì)的溶解性有較大關(guān)系，因此，同樣的固體電極在不同的場(chǎng)合壽命可能差</span> <span style="font-family:宋體">別較大。</span></p><p><span style="font-family:宋體"> 電極不能干放，應(yīng)儲(chǔ)存在相應(yīng)的參比液中，這樣需要重新使用時(shí)，電極馬上就可進(jìn)人工</span> <span style="font-family:宋體">作狀態(tài)。電極如果干放了，在重新使用時(shí)可能不能完成正常校驗(yàn)過(guò)程，需要把電極在相應(yīng)的</span> <span style="font-family:宋體">外參比液中浸泡數(shù)小時(shí)等進(jìn)行處理再重新校驗(yàn)。電極不能儲(chǔ)存在蒸餾水中，否則會(huì)加速外參</span> <span style="font-family:宋體">比介質(zhì)的消耗，降低外參比介質(zhì)的</span>CT<span style="font-family:宋體">濃度，異常增加電極的響應(yīng)時(shí)間。</span></p><p><span style="font-family:宋體"> 變送器的接線端子同樣要保持干凈、干噪，保持密封防止潮濕。防止污染·電纜的中問(wèn)</span> <span style="font-family:宋體">部分意外破損或斷裂必須交給制造商專業(yè)人員檢查維修。</span></p><p> pH<span style="font-family:宋體">值測(cè)量系統(tǒng)的維護(hù)主要的是仔細(xì)閱讀相關(guān)說(shuō)明書(shū)，和制造商專業(yè)技術(shù)人員保持緊密的聯(lián)系，結(jié)合用戶的實(shí)際情況，制定較完善的切實(shí)可行的維護(hù)維修計(jì)劃并認(rèn)真執(zhí)行。</span></p> </div> <div id="tq6ztn8r" class="ly_PrevNext"> <ul> <li>上一篇：<a 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